JOURNAL OF LIGHT INDUSTRY

CN 41-1437/TS  ISSN 2096-1553

亚临界萃取降低烟叶焦油及有害成分研究

田海英,陈伟,董艳娟,李国政,郝辉,周浩,马宇平,聂聪,谷令彪

downloadPDF
田海英, 陈伟, 董艳娟, 等. 亚临界萃取降低烟叶焦油及有害成分研究[J]. 轻工学报, 2015, 30(5-6): 43-48. doi: 10.3969/j.issn.2095-476X.2015.5/6.009
引用本文:田海英, 陈伟, 董艳娟, 等. 亚临界萃取降低烟叶焦油及有害成分研究[J]. 轻工学报, 2015, 30(5-6): 43-48.doi:10.3969/j.issn.2095-476X.2015.5/6.009
shu
TIAN Hai-ying, CHEN Wei, DONG Yan-juan, et al. Study on subcritical extraction technology in reducing tar and harmful components of tobacco leaf[J]. Journal of Light Industry, 2015, 30(5-6): 43-48. doi: 10.3969/j.issn.2095-476X.2015.5/6.009
Citation:TIAN Hai-ying, CHEN Wei, DONG Yan-juan, et al. Study on subcritical extraction technology in reducing tar and harmful components of tobacco leaf[J]. Journal of Light Industry, 2015, 30(5-6): 43-48.doi:10.3969/j.issn.2095-476X.2015.5/6.009
shu

亚临界萃取降低烟叶焦油及有害成分研究

  • 河南中烟工业有限责任公司 技术中心, 河南 郑州 450000;

  • 中国烟草总公司 郑州烟草研究院, 河南 郑州 450001;

  • 郑州大学 物理工程学院, 河南 郑州 450001

    • 通讯作者:马宇平

  • 基金项目:国家烟草专卖局减害重大专项项目(110201301024JH-05)

  • 中图分类号:TS41+1

Study on subcritical extraction technology in reducing tar and harmful components of tobacco leaf

  • Technolgy Center, China Tobacco He'nan Industrial Co., Ltd., Zhengzhou 450000, China;

  • Zhengzhou Tobacco Research Institute of CNTC, Zhengzhou 450001, China;

  • College of Physical Engineering, Zhengzhou University, Zhengzhou 450001, China

    • Corresponding author:MA Yu-ping,
  • Received Date:2015-06-05
    Available Online:2015-11-15

    CLC number:TS41+1

  • 摘要:为探索降焦减害的新途径,从源头上降低卷烟中焦油及有害成分,将亚临界萃取技术引入烟叶的处理过程,对萃取条件进行优化,对用处理后烟丝制成的卷烟中主流烟气的有害成分、焦油、烟碱等释放量进行分析,同时考查处理后烟丝化学成分、加工性能及感官质量的变化情况,结果表明:用二甲醚作萃取溶剂,微波破壁处理然后萃取2次,每次30 min为最优的萃取方式;主流烟气中焦油、烟碱有明显降低,降低比例分别为33.4%和62.2%;处理后烟丝的加工性能无明显变化;7种有害成分中苯酚,HCN,NH 3,CO和B[a]P这5种成分的释放量降低明显,有害指数降低了3.87;感官评吸的柔细度、余味、刺激性均好于对照样,呈现柔、细、甜的特点.这表明,亚临界萃取技术在降低烟叶的焦油和有害成分释放量方面具有重要的应用价值.
    Abstract:In order to investigate the new way to reduce tar and harmful components in cigarette, subcritical extraction technology was used to treat tobacco leaf.The extraction conditions were optimized.The deliveries of the harmful components, tar, nicotine in mainstream smoke of cigarettes prepared with the extracted cut tobacco were determined, the chemical components, processability and sensory quality were also evaluated.The results indicated that:microwave wall-breaking treatment, dimethyl ether extraction 2 times, each time 30 min was the optimal extraction method;the deliveries of tar and nicotine were significantly lowered than the control sample with the decreased rate at 33.4% and 62.2% respectively;the structure of extracted cut tobacco remained no obvious change; in the seven harmful components, the release amount of phenol, HCN, NH 3, CO and B[a]P were decreased.The harmful index reduced by 3.87;the sensory evalution of extracted cut tobacco was found to be superior to the controller in tender degree, aftertaste and stimulation.It was characterized by tenderness and sweetness.The study showed that subcritical extraction technology provides a potential way of reducing tar and harmful components in tobacco leaf.
    1. [1]

      谢剑平,刘惠民,朱茂祥,等.卷烟烟气危害性指数研究[J].烟草科技,2009(2):5.

    2. [2]

      吴殿信,王兵,刘朝贤,等.卷烟降焦技术方法[J].烟草科技,1999(1):7.

    3. [3]

    4. [4]

      Veggi P C,Cavalcanti R N,Meireles M A A.Production of phenolic-rich extracts from Brazilian plants using supercritical and subcritical fluid extraction:Experimental data and economic evaluation[J].Journal of Food Engineering,2014,131:96.

    5. [5]

      Tsuchiya Y,Sako T,Okajima I,et al.Solubility characteristics and selective extraction of jatropha oil by super-and subcritical CO2extraction[J].Journal of Chemical Engineering of JAPAN,2013,46:250.

    6. [6]

      Chen M,Liu T Z,Chen X L,et al.Subcritical co-solvents extraction of lipid from wet microalgae pastes of Nannochloropsis sp[J].European Journal of Lipid Science and Technology,2012,114:205.

    7. [7]

      Monrad J K,Howard L R,King J W,et al.Subcritical solvent extraction of procyanidins from dried red grape pomace[J].Journal of Agricultural and Food Chemistry,2010,58:4014.

    8. [8]

    9. [9]

      郭孝武.超声提取及其应用[M].西安:陕西师范大学出版社,2003.

    10. [10]

      Woodward C F,Eisner A,Haines P G.Pyrolysis of nicotine to myosmine[J].Journal of the American Chemical Society,1944,66(6):911.

    1. [1]

      杜娟,张楠,许自成,戴亚,李东亮,秦璐. 烤烟不同部位烟叶主要化学成分与感官质量的关系. 轻工学报, 2011, 26(2): 16-20.doi: 10.3969/j.issn.1004-1478.2011.02.005

    2. [2]

      徐丽霞,安毅,关体青,杨靖,毛多斌. 不同烘焙条件下白肋烟感官质量与化学成分相关性分析. 轻工学报, 2012, 27(5): 46-50,54.doi: 10.3969/j.issn.2095-476X.2012.05.011

    3. [3]

      高金玲,李书芳,朱国成,魏甲欣. 真空回潮工序对造纸法再造烟叶的质量影响. 轻工学报, 2012, 27(5): 55-58.doi: 10.3969/j.issn.2095-476X.2012.05.013

    4. [4]

      陈凤华,李山,贾春晓,王瑞玲,王莹莹,毛多斌. 响应面法优化烟叶中蔗糖酯的超声波萃取工艺. 轻工学报, 2013, 28(4): 15-19.doi: 10.3969/j.issn.2095-476X.2013.04.004

    5. [5]

      朴洪伟,金勇华,金钟国,姚晓财,陈明,任瑞冰. 甜橙香胶囊滤棒对烟气有害成分及卷烟香气特性的影响. 轻工学报, 2015, 30(3-4): 48-51.doi: 10.3969/j.issn.2095-476X.2015.3/4.011

    6. [6]

      李慧,任宏杰,姚二民. KC-2A膨胀介质对烟丝化学成分和感官品质的影响. 轻工学报, 2011, 26(2): 21-23.doi: 10.3969/j.issn.1004-1478.2011.02.006

    7. [7]

      程传玲,唐琦,汪文良,刘艳芳. 单料烤烟主流烟气中主要酚类化合物及其与感官质量相关性分析. 轻工学报, 2011, 26(1): 5-8.doi: 10.3969/j.issn.1004-1478.2011.01.002

    8. [8]

      王保会,吴键,郭春生,纪朋,朱智志,张峻松. 烟叶热裂解产物的分析研究. 轻工学报, 2013, 28(2): 69-73.doi: 10.3969/j.issn.2095-476X.2013.02.016

    9. [9]

      张颖璞,李桂珍,黄朝章,李巧灵. 不同产地烟叶的热解反应动力学研究. 轻工学报, 2018, 33(2): 55-62.doi: 10.3969/j.issn.2096-1553.2018.02.009

    10. [10]

      李晓,陈科冰,韩明,马雨佳,纪晓楠,楚晗. 质构仪在烟叶力学特性检测中的应用进展. 轻工学报, 2021, 36(3): 63-69.doi: 10.12187/2021.03.008

    11. [11]

      马雨佳,纪晓楠,刘志洋,韩明,李晓,赵晴晴,李劲锋. 烟叶抗破碎指数与物理特性的关联性分析. 轻工学报, 2022, 37(3): 101-107.doi: 10.12187/2022.03.014

    12. [12]

      程华,王乐军,李孟华,齐伟,徐玉琼. 不同型号吸烟机对卷烟主流烟气释放量的影响. 轻工学报, 2013, 28(4): 34-36.doi: 10.3969/j.issn.2095-476X.2013.04.008

    13. [13]

      沈凯,潘凡达,李旭,樊虎,徐超,韩玉峰,詹望成,金浩. 松散润叶筒三维传热传质过程数值模拟. 轻工学报, 2023, 38(5): 96-103.doi: 10.12187/2023.05.013

    14. [14]

      康文功,胡军,帖金鑫,张锐,余翔,马林. 烟草烷烃含量研究. 轻工学报, 2014, 29(3): 40-43.doi: 10.3969/j.issn.2095-476X.2014.03.009

    15. [15]

      牛津桥,晋照普,郭贞贞,张超帅. 茶叶添加量对再造烟叶卷烟烟气酚类有害物质的影响. 轻工学报, 2014, 29(3): 44-47.doi: 10.3969/j.issn.2095-476X.2014.03.010

    16. [16]

      孙胜南,卢真保,赵星宇,林德洪,王学娟,赵世兴,黄艳,杨靖. 超临界CO2萃取两种典型品种烟草净油及其致香成分与感官品质对比研究. 轻工学报, 2023, 38(4): 84-89.doi: 10.12187/2023.04.011

    17. [17]

      邓国栋,姚光明,李晓,乔学义,张玉海,申玉军. 松散回潮工序加工强度对烤烟烟叶感官特性的影响. 轻工学报, 2011, 26(2): 32-35.doi: 10.3969/j.issn.1004-1478.2011.02.009

    18. [18]

      刘兴乐,杨俊鹏,张敦铁,王昊,高颂,闫铁军,庄虎,刘磊. 基于感官品质与常规化学成分的加热卷烟用烟叶原料评价. 轻工学报, 2024, 0(0): 1-8.

    19. [19]

      程向红,刘强,王根发,邱建华,武志勇. 不同干燥强度对香料烟叶丝质量的影响. 轻工学报, 2022, 37(2): 59-64.doi: 10.12187/2022.02.008

    20. [20]

      王春利,朱文辉,文杰,马林. 烟叶糖含量与其感官舒适度的典型相关分析. 轻工学报, 2013, 28(6): 6-8.doi: 10.3969/j.issn.2095-476X.2013.06.002

  • 加载中
WeChat 点击查看大图
计量
  • PDF下载量:139
  • 文章访问数:8386
  • 引证文献数:0
文章相关
  • 通讯作者:马宇平,
  • 收稿日期:2015-06-05
  • 刊出日期:2015-11-15
    通讯作者:陈斌, bchen63@163.com
    • 1.

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索
    田海英, 陈伟, 董艳娟, 等. 亚临界萃取降低烟叶焦油及有害成分研究[J]. 轻工学报, 2015, 30(5-6): 43-48. doi: 10.3969/j.issn.2095-476X.2015.5/6.009
    引用本文:田海英, 陈伟, 董艳娟, 等. 亚临界萃取降低烟叶焦油及有害成分研究[J]. 轻工学报, 2015, 30(5-6): 43-48.doi:10.3969/j.issn.2095-476X.2015.5/6.009
    shu
    TIAN Hai-ying, CHEN Wei, DONG Yan-juan, et al. Study on subcritical extraction technology in reducing tar and harmful components of tobacco leaf[J]. Journal of Light Industry, 2015, 30(5-6): 43-48. doi: 10.3969/j.issn.2095-476X.2015.5/6.009
    Citation:TIAN Hai-ying, CHEN Wei, DONG Yan-juan, et al. Study on subcritical extraction technology in reducing tar and harmful components of tobacco leaf[J]. Journal of Light Industry, 2015, 30(5-6): 43-48.doi:10.3969/j.issn.2095-476X.2015.5/6.009
    shu

    亚临界萃取降低烟叶焦油及有害成分研究

      通讯作者:马宇平
    • 河南中烟工业有限责任公司 技术中心, 河南 郑州 450000;
    • 中国烟草总公司 郑州烟草研究院, 河南 郑州 450001;
    • 郑州大学 物理工程学院, 河南 郑州 450001
    • 收稿日期: 2015-06-05
    • 网络出版日期: 2015-11-15
    基金项目:国家烟草专卖局减害重大专项项目(110201301024JH-05)

    摘要:为探索降焦减害的新途径,从源头上降低卷烟中焦油及有害成分,将亚临界萃取技术引入烟叶的处理过程,对萃取条件进行优化,对用处理后烟丝制成的卷烟中主流烟气的有害成分、焦油、烟碱等释放量进行分析,同时考查处理后烟丝化学成分、加工性能及感官质量的变化情况,结果表明:用二甲醚作萃取溶剂,微波破壁处理然后萃取2次,每次30 min为最优的萃取方式;主流烟气中焦油、烟碱有明显降低,降低比例分别为33.4%和62.2%;处理后烟丝的加工性能无明显变化;7种有害成分中苯酚,HCN,NH3,CO和B[a]P这5种成分的释放量降低明显,有害指数降低了3.87;感官评吸的柔细度、余味、刺激性均好于对照样,呈现柔、细、甜的特点.这表明,亚临界萃取技术在降低烟叶的焦油和有害成分释放量方面具有重要的应用价值.

    English Abstract

    参考文献 (10) 相关文章 (20)

    目录

    /

      返回文章

      网站版权 © 轻工学报编辑部

      地址：河南省郑州市科学大道136号邮编：450001

      本系统由北京仁和汇智信息技术有限公司开发 技术支持：info@rhhz.net